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The Preparation and Preliminary Characterisation of Three Synthetic Andesite Reference Glass Materials (ARM-1, ARM-2, ARM-3) for In Situ Microanalysis
Wu, Shitou1,2; Worner, Gerhard2; Jochum, Klaus Peter3; Stoll, Brigitte3; Simon, Klaus2; Kronz, Andreas2
2019-12-01
Source PublicationGEOSTANDARDS AND GEOANALYTICAL RESEARCH
ISSN1639-4488
Volume43Issue:4Pages:567-584
AbstractThree synthetic reference glasses were prepared by directly fusing and stirring 3.8 kg of high-purity oxide powders to provide reference materials for microanalytical work. These glasses have andesitic major compositions and are doped with fifty-four trace elements in nearly identical abundance (500, 50, 5 mu g g(-1)) using oxide powders or element solutions, and are named ARM-1, 2 and 3, respectively. We further document that sector-field (SF) ICP-MS (Element 2 or Element XR) is capable of sweeping seventy-seven isotopes (from Li-7 to U-238, a total of sixty-eight elements) in 1 s and, thus, is able to quantify up to sixty-eight elements by laser sampling. Micro- and bulk analyses indicate that the glasses are homogeneous with respect to major and trace elements. This paper provides preliminary data for the ARM glasses using a variety of analytical techniques (EPMA, XRF, ICP-OES, ICP-MS, LA-Q-ICP-MS and LA-SF-ICP-MS) performed in ten laboratories. Discrepancies in the data of V, Cr, Ni and Tl exist, mainly caused by analytical limitations. Preliminary reference and information values for fifty-six elements were calculated with uncertainties [2 relative standard error (RSE)] estimated in the range of 1-20%.
Keywordglass reference materials microanalysis sector-field ICP-MS LA-ICP-MS multiple-element quantification
DOI10.1111/ggr.12301
Funding OrganizationNational Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council
WOS KeywordINDUCTIVELY-COUPLED PLASMA ; LA-ICP-MS ; TRACE-ELEMENT ANALYSIS ; LASER-ABLATION MICROPROBE ; ND-YAG LASER ; MASS-SPECTROMETER ; ID-TIMS ; 213 NM ; USGS ; SAMPLES
Language英语
Funding ProjectNational Natural Science Foundation of China[41525012] ; National Natural Science Foundation of China[41903024] ; China Scholarship Council[201306410007]
Funding OrganizationNational Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; National Natural Science Foundation of China ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council ; China Scholarship Council
WOS Research AreaGeochemistry & Geophysics
WOS SubjectGeochemistry & Geophysics
WOS IDWOS:000496159300001
PublisherWILEY
Citation statistics
Document Type期刊论文
Identifierhttp://ir.iggcas.ac.cn/handle/132A11/95775
Collection岩石圈演化国家重点实验室
科技支撑系统
Corresponding AuthorWu, Shitou
Affiliation1.Chinese Acad Sci, Inst Geol & Geophys, Beijing 100029, Peoples R China
2.Gottingen Univ, Geowissensch Zentrum, D-37077 Gottingen, Germany
3.Max Planck Inst Chem, Abt Klimageochem, Postfach 3060, D-55020 Mainz, Germany
First Author AffilicationInstitute of Geology and Geophysics, Chinese Academy of Sciences
Corresponding Author AffilicationInstitute of Geology and Geophysics, Chinese Academy of Sciences
Recommended Citation
GB/T 7714
Wu, Shitou,Worner, Gerhard,Jochum, Klaus Peter,et al. The Preparation and Preliminary Characterisation of Three Synthetic Andesite Reference Glass Materials (ARM-1, ARM-2, ARM-3) for In Situ Microanalysis[J]. GEOSTANDARDS AND GEOANALYTICAL RESEARCH,2019,43(4):567-584.
APA Wu, Shitou,Worner, Gerhard,Jochum, Klaus Peter,Stoll, Brigitte,Simon, Klaus,&Kronz, Andreas.(2019).The Preparation and Preliminary Characterisation of Three Synthetic Andesite Reference Glass Materials (ARM-1, ARM-2, ARM-3) for In Situ Microanalysis.GEOSTANDARDS AND GEOANALYTICAL RESEARCH,43(4),567-584.
MLA Wu, Shitou,et al."The Preparation and Preliminary Characterisation of Three Synthetic Andesite Reference Glass Materials (ARM-1, ARM-2, ARM-3) for In Situ Microanalysis".GEOSTANDARDS AND GEOANALYTICAL RESEARCH 43.4(2019):567-584.
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